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GCMS results for sample AE07766, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07766 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046864–000046889

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 11:11:01 2002 Quant Results File: 041202SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Apr 16 11:10:55 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 4582173 40.00 ug/L 0.00 10) Napthalene-d8 13.49 136 17504334 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 10194654 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 15803460 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 13045760 40.00 ug/L -0.02 43) Perylene-dl2 34 .79 264 8864754 40.00 ug/L -0.01

System Monitoring Compounds 2 7) TCMX 20.60 207 395663 7.00 ug/L 0.00 Spiked Amount 8.000 Recovery = 87.50%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 07766.D 041202SCAN.M Tue Apr 16 11:11:50 2002 Page 1

NYC-WTC_000046867

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NYC-WTC_000046867Source: NYC Law Department, mirrored locally

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