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GCMS results for sample AE08070, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08070 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046855–000046863

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020415\08070.D Vial: 27 Acq On : 16 Apr 2002 8:02 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:58:35 2002 Quant Results File: 041202SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Tue Apr 16 11:14:47 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 4470887 40.00 ug/L -0.01 10) Napthalene-d8 13.48 136 17044256 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 9947989 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 15452230 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 12060552 40.00 ug/L -0.02 43) Perylene-dl2 34.79 264 8108464 40.00 ug/L -0.02

System Monitoring Compounds 2 7) TCMX 20.60 207 364889 6.61 ug/L 0.00 Spiked Amount 8.000 Recovery = 82.63%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08070.D 041202SCAN.M Tue Apr 16 13:58:47 2002 Page 1

NYC-WTC_000046857

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NYC-WTC_000046857Source: NYC Law Department, mirrored locally

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