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GCMS results for sample AE08069, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08069 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046841–000046854

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020415\08069.D Vial: 26 Acq On 16 Apr 2002 7:13 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:57:03 2002 Quant Results File: 041202SCAN. RE

Quant Method C:\MSDCHEM\l\METHQDS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Last Update Tue Apr 16 11:14:47 2002 Response via Initial Calibration DataAcq Meth 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.98 152 4793694 40.00 ug/L -0.01 10) Napthalene-d8 13.48 136 18089520 40.00 ug/L -0.01 17) Acenapthalene-dlO 18.63 164 10540816 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 16026281 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 12894513 40.00 ug/L -0.02 43) Perylene-dl2 34.79 264 9071295 40.00 ug/L -0.01

System Monitoring Compounds 2 7) TCMX 20.60 207 369360 6.32 ug/L 0.00 Spiked Amount 8.000 Recovery = 79.00%

Target Compounds Qvalue 41) Bis(2-ethylhexyl)phthalate 31.46 149 102771 0.50 ug/L # 90

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08069.D 041202SCAN.M Tue Apr 16 13:58:25 2002 Page 1

NYC-WTC_000046843

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NYC-WTC_000046843Source: NYC Law Department, mirrored locally

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