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GCMS analysis results, Sample AE08267, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08267 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048421–000048435

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048423
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020417\08267.D Vial: 24 Acq On : 18 Apr 2002 4:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 18 10:00:17 2002 Quant Results File: 041702SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu Apr 18 09:38:13 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 7912200 40.00 ug/L - 0.02 10) Napthalene-d8 13.49 136 30279644 40.00 ug/L -0.03 17) Acenapthalene-dlO 18.63 164 16402783 40.00 ug/L -0.02 29) Phenanthranene-dlO 23.02 188 25227348 40.00 ug/L -0.02 37) Chrysene-dl2 30.89 240 18581796 40.00 ug/L -0.05 43) Perylene-dl2 34.79 264 12122104 40.00 ug/L -0.02

System Monitoring Compounds 2 7) TCMX 20.60 207 657654 7.23 ug/L 0.00 Spiked Amount 10.000 Recovery = 72.30%

Target Compounds Qvalue 41) Bis(2-ethylhexyl)phthalate 31.46 149 87211 0.24 ug/L # 91

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08267.D 041702SCAN.M Thu Apr 18 14:08:42 2002 Page 1

NYC-WTC_000048423

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NYC-WTC_000048423Source: NYC Law Department, mirrored locally

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