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GCMS analysis results, Sample AE08264, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048355–000048377

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 18 09:51:23 2002 Quant Results File: 041702SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu Apr 18 09:38:13 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 7982073 40.00 ug/L -0.02 10) Napthalene-d8 13.49 136 30812945 40.00 ug/L -0.03 17) Acenapthalene-dlO 18.63 164 16859480 40.00 ug/L -0.02 29) Phenanthranene-dlO 23.02 188 26030431 40.00 ug/L -0.02 37) Chrysene-dl2 30.89 240 19644361 40.00 ug/L -0.05 43) Perylene-dl2 34.79 264 13892082 40.00 ug/L -0.01

System Monitoring Compounds 27) TCMX 20.60 207 646482 6.92 ug/L 0.00 Spiked Amount 10.000 Recovery = 69.20%

Target Compounds Qvalue 35) Di-n-butylphthalate 25.16 149 71540 0.09 ug/L # 93

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08264.D 041702SCAN.M Thu Apr 18 14:08:19 2002 Page 1

NYC-WTC_000048357

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NYC-WTC_000048357Source: NYC Law Department, mirrored locally

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