GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 2-Butene, 1-bromo-3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

4.53 22.13 ug/L 14567200 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Butene, 1-bromo-3-methyl- 148 C5H9Br 000870-63-3 83 2 2-Methyl-4-bromo-l-butene 148 C5H9Br 020038-12-4 83 3 2-Butene, 1-bromo-3-methyl- 148 C5H9Br 000870-63-3 72 4 Geranyl nitrile 149 C10H15N 101660-61-1 56 Abundance Scan 247 (4,530 min): 08068 D (-239) (-) m/z 69.30 100.00% 69 41

5000

' ................ । । । i ■ । । ■ । । । 53

n/z-> 01 TIPWPITTT 10 20 30 40 *2+ 50 60 70 81 93 107 119 TWTIIOIIOIPmmmmn 133 148 80 90 100 110 120 130 140 150 m/z 4 20 4 40 41.30 ft 4.60 4.80 78.87% Abundance #108781 2-Butene, 1-bromo-3-methyl- 41 69

5000- r-j-r r T 4.20 4.40 4 60 4.80

27 m/z 39.30 19.68% 53 150 01 TTTTTTT —llerr, 1‘Ji-,. । .-.-■■i — 111WTINITPTLTTTTTII Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #22284 2-Methyl-4-bromo-1-butene 69 —, , । , . , Q , ,, । . . . r, , i , , । 41 4 20 4.40 4.60 4.80 5000 m/z 53.30 11.63% 55 27 148 ..................... ........ , 01 Tt ' i —4 - - n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #108782: 2-Butene, 1-bromo-3-methyl- iviimea p । । > । । । . । । 41 60 4.20 4.4 0 4 6 0 4.80 m/z 67.30 6.54%

5000 27 53 150

/z-> 0- 19— 34 4— —42470—— 8081 9093 100 107110 119 TTyr 10 20 30 40 50 60 133 N 120 130 140 150 ■ r111' । ■' ■11 ■ ■111 ■11' ।1 ■ ■111 ■111'1'111 ■ ■ ■ । ■ ■ । ' 1 1 G 1 1 ■ ■ ........ 1 1 ' 1 i 4.20 4.40 4.60 4 80

08068.D 041202SCAN.M Tue Apr 16 13:56:50 2002 Page 6

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