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GCMS analysis results for sample AE07316, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07316 conducted on April 10, 2002.

NYC-WTC_000046655–000046663

Folder label: “GCMS X 3/28/02 A 2/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APRO 3 02\7316.D Vial: 12 Acq On 3 Apr 2002 11:34 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

14.84 1.52 ug/1 209915 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 2 Phenethyl mine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzenee hanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 4 N-(Trif/uoroacetyl)-N /O,OI,0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 32 Abundance Scan 1067 (14.842 min): 7316.D (-) m/z 73.00 100.00% 73

5000 267 355 1 1 i ■ ‘ 1 117l ’ 111 14.60 14.80 15.00 15.20 45 103118133 154 177 193 223 251 |.... 323339 | 0 i । ।I । i । । । । i-i । । । r r । ‘i i । ii <1 r । । ii ii । । । ’ । r । r 1 i ■ । n' ‘ i11" i1 ,ri i ■11 ’I’’’ TITUTTWTTLTTTTTTT m/z 267.00 42.08% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 I 1 ' 14.60 14.80 15.00 15.20 m/z 355.05 40.38% r-q-m-rp- 191 207 i ■ ■ ■ ■ i ■ - ■11 i",v 11 ’T’ 11 323339 TTTE—mm ITT 2511 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73

14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.10% 44 ...................................................................... ........294 .......... m/z-> , 88 ITT 130147 193 267 1 i 1′1 i r | > i i T [ i I i i । । i i I । i ′′′ [ > > > > [i i i i | , > < < | I FiU ।

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ii i i | > i i i | i >■ i | i i I'l | I I I I | I h Abundances #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ' ' I 1 1 1 ' r1 ' ' 1 I ' 1 ' 1 1 1 ' 73 14.60 14.80 15.00 15.20 m/z 268.00 12.31% 5000 267 44 151 179194209 1111′1171701 TTTTUOT 250 1’111111111111111111’1’11—17’01’ ......... I\............ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

7316.D GCMS0403.M Tue Apr 09 13:08:44 2002 Page 1

NYC-WTC_000046662

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NYC-WTC_000046662Source: NYC Law Department, mirrored locally

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