GCMS reference analysis results for sample AE07311, April 2002

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Laboratory report presenting GCMS reference analysis for sample AE07311 conducted on April 3, 2002, with measured values and MDLs.

NYC-WTC_000046578–000046602

Folder label: “GCMS X 3/28/02 A 2/27/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR1302\1965.D Vial: 3 Acq On : 13 Mar 2002 12:01 pm Operator : Sample : re-extraction Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 27 11:54 2002 Quant Results File: GCMS0208. S

Quant Method C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Response via DataAcq Meth Wed Feb 27 11:30:15 2002 Initial Calibration GCMS0308 ft9' Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.31 152 429995 20.00 ug/1 -0.05 10) Naphthalene-d8 15.93 136 1697559 20.00 ug/1 -0.06 17) Acenaphthene-diO 21.25 164 909770 20.00 ug/1 -0.06 29) Phenanthrene-diO 25.69 188 1411415 20.00 ug/1 -0.07 38) Chrysene-dl2 33.76 240 1154199 20.00 ug/1 -0.08 44) Perylene-dl2 38.03 264 852487 20.00 ug/1 -0.09

System Monitoring Compounds 37) 2,4-DDD 30.77 235 71477 4.85 u 0.27 Spiked Amount 5.000 Recovery 97.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.55 93 170 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.00 128 379 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.72 149 1297 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 1965.D GCMS0208.M Wed Mar 27 11:55:46 2002 Page 1

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