GCMS analysis results for sample AE03507, March 29 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\3507.D Vial: 22 Acq On ; 22 Mar 2002 7:59 am Operator: Sample : re-extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 10:38 2002 (Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 801206 20.00 ug/1 -0,09 10) Naphthalene-d8 15.91 136 3176925 20.00 ug/1 -0.09 17) Acenaphthene-dlO 21.22 164 1721272 20.00 ug/1 -0.10 29) Phenanthrene-dlO 25.67 188. 2601822 20.00 ug/1 -0.10 38) Chrysene-dl2 33.73 240 1582972 20.00 ug/1 -0.12 44) Perylene-dl2 37.99 264 903912 20.00 ug/1 -0.13

System Monitoring Compounds 37) 2,4-DDD 30.74 235 97022 5.13 ug/mL 0.24 Spiked Amount 5.000 Recovery = 102.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93' 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.96 128 216 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chlorohaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.64 165 105 N.D. 25) Diethylphthalate 22.69 149 679 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd o:oo 77 0 N.D.

{#) = qualifier out of range (m) = manual integration 3507.D GCMS0308.M Mon Mar 25 10:42:20 2002 Page 1

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