GCMS analytical results for sample AE03832, March 29, 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR2202\3832.D Vial: 13 Acq On 23 Mar 2002 5:55 am Operator: Sample gc/ms scan 2/20 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 26 14:43 2002 Quant Results File: GCMS0308.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Tue Mar 26 14:13:06 2002 Response via Initial Calibration DataAcq Meth GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.27 152 389548 20.00 ug/1 -0.09 10) Naphthalene-d8 15.90 136 1525107 20.00 ug/1 -0.10 17) Acenaphthene-diO 21.21 164 829241 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.65 188 1220017 20.00 ug/1 -0.11 38) Chrysene-dl2 33.71 240 746540 20.00 ug/1 -0.13 44) Perylene-dl2 37.96 264 444551 20.00 ug/1 -0.16

System Monitoring Compounds 37) 2,4-DDD 30.73 235 81933 + 8.20ug/mL 0.23 Spiked Amount 5.000 Recovery = 164.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chlorppropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.62 82 279 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 . N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.69 149 572 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 3832.D GCMS0308.M Tue Mar 26 14:44:43 2002 Page 1

NYC-WTC_000038095