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GCMS analytical results for sample AE03832, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03832 analyzed on March 29, 2002.

NYC-WTC_000038093–000038101

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2202\3832.D Vial: 13 Acq On : 23 Mar 2002 5:55 am Operator: Sample : gc/ms scan 2/20 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 2614:432002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Mar 26 14:13:06 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0:00 178 0 N.D. 34) Anthracene 25.66 178 206 N.D. 35) Di-n-butylphthalate 27.63 14 9 3264 N.D. 36) Fluoranthene 0.00 2 02 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.16 . 149 411 N.D. 41) Benzo(a)anthracene 33.72 228 1667 N.D. 42) Bis(2-ethylhexyl)phthalate 33.92 149 8110 0.27 ug/1 95 43) Chrysene 33.72 228 1667 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.77 252 109 N.D.' 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.97 252 1852 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 3832 .D GCMS0308.M Tue Mar 26 14:44:46 2002 Page 2

NYC-WTC_000038096

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NYC-WTC_000038096Source: NYC Law Department, mirrored locally

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