NYC-WTC_000012363
Gas chromatography-mass spectrometry results for sample AE04449 analyzed on April 4, 2002.
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GCMS analysis report, sample AE04450, April 2002
Machine-extracted title · confidence 100%Gas chromatography-mass spectrometry results for sample AE04450 analyzed on April 4, 2002.
NYC-WTC_000012372–000012380Folder label: “GCMS X 3-1-02 A 3-21-02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2102\4450.D Vial: 13 Acq On : 21 Mar 2002 11:07 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 9:28 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.26 152 591699 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 2296340 20.00 ug/1 -0.09 17) Acenaphthene-diO 21.22 164 1236831 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1850896 20.00 ug/1 -0.11 38) Chrysene-dl2 33.72 240 1144035 20.00 ug/1 -0.12 44) Perylene-dl2 37.97 264 637419 20.00 ug/1 -0.15
System Monitoring Compounds 37) 2,4-DDD 30.74 235 75923 5.64 ug/mL 0.24 Spiked Amount 5.000 Recovery = 112.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.30 146 441 N.D. 5) 1,4-Dichlorobenzene 12.30 146 441 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.96 128 355 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.53 165 311 N.D. 25) Diethylphthalate 22.69 149 339 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 4450.D GCMS0308.M Fri Mar 22 09:33:16 2002 Page 1
NYC-WTC_000012374
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