GCMS analysis report, sample AE04420, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAR2102\4420.D Vial: 11 Acq On : 21 Mar 2002 9:08 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 22 9:07 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.26 152 556689 20.00 ug/1 -0.09 10) Naphthalene-d8 15.91 136 2177411 20.00 ug/1 -0.09 17) Acenaphthene-dl0 21.21 164 1165413 20.00 ug/1 -0.10 29) Phenanthrene-diO 25.66 188 1741143 20.00 ug/1 -0.10 38) Chrysene-dl2 33.73 240 1108424 20.00 ug/1 -0.12 44) Perylene-dl2 37.98 264 681160 20.00 ug/1 -0.15

System Monitoring Compounds 37) 2,4-DDD 30.73 235 70540 5.57 ug/mL 0.23 Spiked Amount 5.000 Recovery = 111.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichiorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.60 82 982 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.95 128 194 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.54 165 207 N.D. 25) Diethylphthalate 22.69 149 215 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4420.D GCMS0308.M Fri Mar 22 09:13:38 2002 Page 1

NYC-WTC_000012355