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GCMS analysis results, sample AE10808, May 2002

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AE10808 performed May 17, 2002, including unknown compound detection and surrogate recovery testing.

NYC-WTC_000046372–000046381

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046377
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0802\10808.D Vial: 23 Acq On 9 May 2002 8:08 am Operator: Sample GC/MS SCAN 5/7 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.159 336 340 346 rBV 509865 992584 28.42% 5.619% 2 12.191 775 780 797 rVB 1097581 2478776 70.97% 14.033% 3 14.793 1059 1064 1070 rVB 125995 244740 7.01% 1.386% 4 15.829 1171 1177 1195 rBV 1504936 3117686 89.26% 17.650% 5 21.135 1749 1756 1777 rBV 1676922 3492641 100.00% 19.773%

6 23.270 1982 1989 1998 rVB2 187287 394607 11.30% 2.234% 7 25.579 2234 2241 2252 rBV2 1459530 3161278 90.51% 17.897% 8 33.634 3113 3120 3141 rBV2 994056 2203373 63.09% 12.474% 9 37.858 3573 3581 3602 rBV2 520445 1578394 45.19% 8.936%

Sum of corrected areas: 17664079

10808.D GCMS0507.M Fri May 10 08:21:21 2002

NYC-WTC_000046377

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NYC-WTC_000046377Source: NYC Law Department, mirrored locally

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