GCMS analysis results for sample AE09587, May 2002

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Library Search Compound Report Data File C : \HPCHEM\ 1\DATA\MAYO 802\9587.D Vial: 20 Acq On 9 May 2002 5:10 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.80 2.10 ug/1 175708 Naphthalene-d8 15.82 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopen siloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 Pheneth amine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 3,4-Di droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 4 Benze ethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1065 (14796 min): 9587.D (-) m/z 73.10 100.00% 73 fl 5000 267 355 TIT 45 14.40 14.60 14.80 15.00 15.20 133 154 177 193 323339 1 223 "I i j r |r । । । । । । TIUmT ।251 103 TTITITTT . ’ ’I [ ’* ’ 11’1’1’17’11*11111’111 ’ 1 । r, m/z 267.05 35.21%| m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 .......... . 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 34.72%

m/z->_____ 40 r 1 1 1 i ' r ' 111 1' 11 i ■ ■1 ’ i ■'1 11 323339 191207 TTTTP I 11 11 I ‘-' I 60 80 100 120 140 160 180 200 220 _ 240 260 280 300 320 340 360 21—— Abundance #74239: Phenethylamine, N-methyl-beta.,3,4-tris(trimethyls 7)3 | | I I I I | I I I I । \ I I । । i i i i । i r

14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 12.24% ■

44

88 130147 193 267 294 ‘' 111 ’ 1’1 ,TI 11 ' | | | । ' । | | | I I | i i i i | i i r i ( i i r i । i i i i [ । i r f | I I I I | "I *I I I j I I I 'l | I I I I | 1' sak. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- .................. ■ i ■ ■ ■ ■ । \...................... । i ■ ■ ■ ■ । । । 1 । t । । 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 9.51%

5000 267 179 356 45 147 209 237 312 341 1 11111•1r i'' ‘1 r 1111''111 • ■11111 'r i1'11 r 1' ■ i1 ‘'11 ri 111111 ‘ r 1'11ri 111111 TTTT .................. \...................... ' I 1 1 ' 1 i ' ■ ■ 1 i 1 1 1 1 i 1 1 1 1 | ' 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9587 ,D GCMS0507.M Fri May 10 08:23:00 2002 Page 2

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