GCMS analysis results for sample AE10519, May 2002

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GCMS analytical report for sample AE10519 focusing on unknown compounds from May 21, 2002.

NYC-WTC_000045353–000045363

Folder label: “GCMS X 5/2/02 A 5/12/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY1002\10519.D Vial: 42 Acq On : 12 May 2002 6:03 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Benzene, 1,2,3,5-tetrachloro-4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. > .24 3.36 ug/1 426587 Phenanthrene-dl0 25.55 it# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1/2,3,5-tetrachloro-4,6-di 242 C8H6C14 000877-09-8 95 2 Benzene, 1,3,5-trichloro-2-(1-methy 222 C9H9C13 054965-70-7 38 3 Benzaldehyde, 2,4,5-trichloro- 208 C7H3C130 035696-87-8 25 4 Quinoline, 2-chloro-6-methoxy-4-met 207 C11H10C1NO 006340-55-2 12 Abundance 7 Scan 1986 (23.242 min): 10519.D (-) 207 m/z 206.95 100.00%

244 5000-

75 85 , 99 121 136 171 J. 39 50 61 23.00 23.20 23.40 23.60 ,7 l , II +41,319,. ., 146157 .A182193.. —229 ill+r , ' 1 I 11 ‘ ' I ' 1,1 p । । i ] r m/z 208.95 96.07% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32224: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207

244 5000- J lT 1r‘‘II ‘TT 136 23.00 23.20 23.40 23.60 m/z 243.95 65.46% 49 ........I.......... 73.1 9 171 -L i i i i [ i pl i | | i i i | r N 1 1 ‘ i 1 ' 1 1 1 1 ' m/z->_______ 40 60 80 100 120 140 160 .180 200 220 240 Abundance #27962: Benzene, 1,3,5-trichloro-2-(1-methylethyl)- 207 ............. "I I ] I I I I | I I ! I ] I I I I | I T

23.00 23.20 23.40 23.60 5000 m/z 241.90 50.98% 222 136 171 194

i i | । > । i ] । । j । ] । । 1 । i । । । । [ r 1‘‘‘I‘‘‘IUUU TT +1’ ............ 11 1 T m/z-> 40 60 80 100 120 140 160 180 200 220। 240 Abundance #24688: Benzaldehyde, 2,4,5-trichloro- ....... J............ "I i | i । i 1 i r m । i i i i । j r 209 23.00 23.20 23.40 23.60 m/z 136.00 32.77% 5000

109 , 179 । 145 ....................... I................ ' 1-11 1 1 1 1 ' - । । | । ii । | i i । । ] i t i i । i m i । । i । । । r r i i । i 1 ■ i 1 r m/z—> 40 60 80 100 120 140 160 180 200 220 240 23.00 23.20 23.40 23.60

10519.D GCMS0510.M Thu May 16 15:34:35 2002 Page 3

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GCMS analysis results for sample AE10522, May 2002 · Box DEP Box 25

NYC-WTC_000045386

GCMS analytical report for sample AE10522 showing unknown compounds and surrogate recovery data from May 22, 2002.

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