GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 3-Buten-2-ol, 2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

4.96 0.37 ug/L 368965 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18- 83 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 3 Butenol, methyl- 86 C5H10O 060766-00-9 59 4 Furan-2-carbonyl chloride, tetra... 134 C5H7C1O2 052449-98-6 53 Abundance Scan 319 (4.954 min): 9093. D (-313) (-) m/z 71.10 100.00% 43 71

5000 59 39 55 rrrf .... R......... 1 I I I I I-1 I I I I I [“I I I.... I "TI

Ol I 1 I I I I I I I I 1 I I ।111' । T al + 501 11131111117 67 i 86 । I n । । i i i i i” m/ z 4.60 4.80 43.10 5.00 520 94.56% 5.40

L. _ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #114555: 3-Buten-2-ol, 2-methyl- 43 71 WWwow

5000 59 4.60 4.80 5.00 5.20 5.40 27 31 39 m/ z 41.10 61.51% 53

m/z-> 01 v 5 1518 j ! I ! ! p I I ! | ! ! I I,I — —

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 + 45QL56 IH 671 86 I I I j . I I I | ! I I I | I I ,! | I I I I |

Abundance #114557: 3-Buten-2-ol, 2-methyl- 71 43 AAorw-W WW/wIn V I I I I I I I I I ill I I I 1 1 P I I I I U

460 4.80 5.00 5.20 5.40 5000 m/z 59.10 37.70% 59

27 31 39

m/z-> 01 Ti 5 ‘‘‘1, | ! । I I | । I ! ! 36 TH+ 505356 1111111 I 67 86

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #++ + -H + + Abundance #24435: Butenol, methyl- A M AA I I , , ,I I JIAI I I I I I I I I 43 71 460 4.80 5.00 5.20 5.40 m/ z 69.10 33.13%

5000 59 27 15 31 39 53

m/z-> 12, 18 0 ‘ I’’ I I | I I I I 5 24) , IIITT T i-l -p I T t | I I

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 36. TTH + 46.50.1.5611 63 67, ,74 79 8386 1 I 1 I ] I I II I I I I I I I I I I I I I I I f I I I I I f I I I

4.60 4.80 5.00 5.20 5.40

9093.D 050102.M Thu May 09 13:33:18 2002 Page 4

NYC-WTC_000044910

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NYC-WTC_000044025

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