GCMS analysis results, sample AE09969, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050602\9969.D Vial: 26 Acq On 7 May 2002 8:03 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 4.94 0.33 ug/L 254434 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 50 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-445 4 2(3H)-Furanone, dihydro-3-hydrox... 130 C6H10O3 052126-90-6 38 Abundance Scan 317 (4.942 min): 9969.D (-311) (-) m/z 7i.io ~A6b .oo%| 71 43

5000 4C

4। 49 55 59

. 67 ) । । । । ■, । I । r i,... 84 88 .... AM

m/z 4.60 4.80 L 5.00 5.20 1 । । 1 । 1

‘117 1 ' ' I ' ' ' ' ] ' 1 ' ' 1 1 ' ' ’ I y । < 1111111 <11111111111 ■■ 11 ■ 43.10 82.45% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114555: 3-Buten-2-ol, 2-methyl- 71 43 AWMAyyM

5000 ■ ' i 1 59 4.60 4.80 5.00 5.20 27 31 39 m/z 41.10 62.04% 1518 53 .. | 671 86 l " 1' i ■ rTI > rl । । । । । । । I — — 111159.1,561/.. rr 11 I I i | 1 I i i | I Fi j I i I I | i i i t |

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114556: 3-Buten-2-ol, 2-methyl-

43 71 AANJU 4.60 4.80 5.00 5.20 5000 m/z 40.10 38.77% 59 27 31 39 53 |llll|l...... 11111 174 ■ i' । • > • > । 86 +50 156163,67+ ' 11 ■ > ■ । ■r । ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #114557: 3-Buten-2-ol, 2-methyl- 1 ■ i 1 43 7 460 4.80 5.00 5.20 m/z 59.10 36.53% 5000 59

n/z-> „ . 5953561,, 67 mH 27I . 31I 439 86 50 I > ' I I I I I j ITTni I I I r I I I I I I I I I I I I I 4

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 I I r । । । > r । । । । r | I': । । ] ■] ri 3 । i i . ..... .... ..1 1 1 1 1 4.60 1 ' 1 1 1 ' 1 • I 1 I ' I 4.80 5.00 5.20 I I ' I 1 I I

9969.D 050102.M Tue May 07 15:48:35 2002 Page 5

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