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GCMS analysis results for sample AE10161, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE10161 conducted on May 10, 2002.

NYC-WTC_000044815–000044826

Folder label: “GCMS X 4/29/02 A 5/3/02

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Scanned page image, NYC-WTC_000044822
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 6 02\10161.D Vial: 9 Acq On 8 May 2002 1:40 am Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propane, 1-nitro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.03 0.62 ug/1 40602 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 1-nitro- 89 C3H7NO2 000108-03-2 12 2 2-Butenal, (E)- 70 C4H60 000123-73-9 9 3 Cyanic acid, ethyl ester 71 C3H5NO 000627-48-5 9 4 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 9 Abundance / Scan 217 (7.030 min): 10161 .D (-) m/ z 41.05 100.00% 41 71

5000 55 59 adyAAA— 4 6.60 6.80 7.00 7.20 7.40 HH 450 .,1 86 38 67 I I I I I I I I I I I I I I I I I — TTI000110110011010111 m/ z 43.05 96.22% l1 " 11' i *1111'1" r TT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62970: Propane, 1-nitro- 27 43

5000 39 6.60 6.80 7.00 7.20 7.40 30 m/ z 71.10 70.81% 15 | > ! ■ ■ | I I ! I । < I ! > | ! ! ! ! | । ,46 111"11" " ।। i" " i11" r 1 " i n " ।11'11 ■ ‘1' । m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62443: 2-Butenal, (E)- 41 70 A 1 i 1 1 1 ' r 11unni 1 6.60 6.80 7.00 7.20 7.40 5000 27 m/ z 69.05 67.14% 38

33 48 55 TTTT i1'11111 r ‘ i1' " i'1' ■ i " i " '' i' i11 " i " 1' 11 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #237: Cyanic acid, ethyl ester I I I I I I I I I I I I I WAA i I A I I I I 29 6.60 6.80 7.00 7.20 7.40 m/z 59.10 35.76% 56 5000 71

28 43

m/z-> i11111 5 ’ ’’ I 4 40, | 1———100110101000100017 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 1’1 111" i 6.60 6.80 7.00 7.20 7.40

10161.D GCMS0507.M Thu May 09 11:12:45 2002 Page 1

NYC-WTC_000044822

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NYC-WTC_000044822Source: NYC Law Department, mirrored locally

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