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GCMS reference standard results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Reference standard analysis data for volatile organic compounds used to verify gas chromatography-mass spectrometry accuracy.

NYC-WTC_000044770–000044777

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\APR2502\REF2.D Vial: 5 Acq On : 25 Apr 2002 4:38 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 7:38 2002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.69 284 150605 12.94 ug/1 # 92 34) Phenanthrene 25.65 178 614969 11.75 ug/1 99 35) Anthracene 25.79 178 534876 10.39 ug/1 99 36) Di-n-butylphthalate 27.56 149 752233 11.49 ug/1 100 37) Fluoranthene 29.28 202 587045 11.15 ug/1 96 40) Pyrene 29.95 202 601829 11.51 ug/1 98 41) Butylbenzylphthalate 32.08 149 252061 9.86 ug/1 95 42) Benzo(a)anthracene 33.59 228 401719 11.07 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 325069 9.93 ug/1 99 44) Chrysene 33.72 228 435789 12.11 ug/1 98 46) Di-n-Octylphthalate 35.60 149 361073 7.58 ug/1 # . 99 47) Benzo(b)fluoranthene 36.69 252 347483 11.29 ug/1 96 48) Benzo(k)fluoranthene 36.76 252 354860 11.84 ug/1 98 49) Benzo(a)pyrene 37.68 252 212769 8.38 ug/1 97 50) Indeno(1,2,3-cd)pyrene 41.95 276 223468 8.75 ug/1 95 51) Dibenz(a,h)anthracene 42.03 278 195257 10.02 ug/1 96 52) Benzo(g,h,i)perylene 43.17 276 192457 9.02 ug/1 97

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0412.M Fri Apr 26 07:38:51 2002 Page 2

NYC-WTC_000044776

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NYC-WTC_000044776Source: NYC Law Department, mirrored locally

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