GCMS analysis results for sample AE08756, May 2002

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Laboratory report documenting GCMS analysis of sample AE08756 conducted on May 8, 2002.

NYC-WTC_000044731–000044747

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

- Data File C:\MSDCHEM\1\DATA\050202\8756.D Vial : 15 Acq On 2 May 2002 11:05 pm Operator: Mclean Sample 4/29 re-ext Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 2-Propenoyl chloride Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

3.80 0.23 ug/L 165524 1,4-Dichlorobenzene-d4 9.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenoyl chloride ’ 90 C3H3C10 000814-68-6 1. 2 Nitrosyl chloride 65 CINO 002696-92-6 1 3 Propanoyl chloride 92 C3H5C1O 000079-03-8 1 4 1,3-Diamino-2-propanol 90 C3H10N2O 000616-29-5 1 Abundance Scan 123 (3.802 min): 8756.D (-121) (-) m/z 40.10 100.00% 40

5000 35 84 ■ i ' 1 1 ’ i 1 1 ' ■ i 1 ■ 1 ' i 1 1 1 1 i 1 ' 49 3.40 3.60 3.80 4.00 4.20 ■ । Li i i i ।। ~ । । । । । । । |~“i r II I IIII I IIplI I I I I I I I I I I I I I I I m/z 3 5.10 45.47% m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #60: 2-Propenoyl chloride 27 55

5000 । iiii । I । । [ । । । r । r 101010 ' r

3.40 3.60 3.80 4.00 4.20 m/z 84.00 35.40%

n/z-> Abundance .................. .. | 1 1 [ 1 > 1 1 । 1 1 1 1 । 1 ■ 0 10 20 +440,45,50.. , , 63,67 72 77 83 90........ 30 40 50 #713: Nitrosyl chloride trTl’i ' | I ' i i i । । । i r | | । 1 i । । 60 70 80 90 100 4- 3b

3.40 3.60 3.80 4.00 4.20 5000

। 1 ■ ■ 1 । 1 1 1 1 । 1 ■ 14 1 35

' ■ ' 1 i 1 ' ' ■ i 1 ■ ' r i ' ' 1 ■ i ' 1 ■ 1 i ' 1 ' 1 i rrB । ■' wmhein m/z 4 9.10 12.30%

Tl/Z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #472: Propanoyl chloride 29 3.40 3.60 3.80 4.00 4.20 57 m/z 86.00 10.68% 5000 owwy"Hy*=t i i [ 2. 14 , , 24 r—i i k i ii । । । । r 35 42 49 65 71 76 82 | । । H11111 ‘ r— r" ।11■।1111 T1 I’ii i । >< । । । । । । । । । । —i ] r 91 I I I I I I I I I I I I I I_I I l l * I I I

/z-> 0 10 20 30 40 50 60 70 80 90 100 3.40 3.60 3.80 4.00 4.20

8756.D 050102.M Mon May 06 14:02:57 2002 Page 5

NYC-WTC_000044739

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NYC-WTC_000044739Source: NYC Law Department, mirrored locally

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