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GCMS analysis results for sample AE09335, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09335 conducted on May 8, 2002.

NYC-WTC_000044672–000044699

Folder label: “GCMS X 4/29/02 A 5/3/02

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Scanned page image, NYC-WTC_000044674
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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\l\DATA\050202\9335.D Vial: 13 Acq On 2 May 2002 9:27 pm Operator: Mclean Sample 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 06 13:58:56 2002 Quant Results File: 050102.RES Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) ( Title : 508 Modified GC/MS scan QR/ 1 (P Last Update : Mon May 06 12:20:41 2002 AM • Response via : Initial Calibration (W _ Va DataAcq Meth : 508SCAN wOPP Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.94 152 6270011 40.00 ug/L 0.01 10) Napthalene-d8 13.44 136 25364421 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.58 164 13861514 40.00 ug/L 0.01 29) Phenanthranene-dlO 22.97 188 20625459 40.00 ug/L 0.01 37) Chrysene-dl2 30.82 240 17104718 40.00 ug/L 0.01 43) Perylene-dl2 34.73 264 12622377 40.00 ug/L 0.02

System Monitoring Compounds 2 7) TCMX 20.54 209 703481 7.23 ug/L 0.00 Spiked Amount 10.000 Recovery = 72.30% 50) 2,4-ddd 0.00 235 0 0.00 ug/L Spiked Amount 5.000 Recovery 0.00%

Target Compounds Qvalue 41) Bis(2-ethylhexyl)phthalate 31.40 149 337699 0.80 ug/L # 91

(#) = qualifier out of range (m) = manual integration (+) = signals summed 9335.D 050102.M Mon May 06 13:59:17 2002 Page 1

NYC-WTC_000044674

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NYC-WTC_000044674Source: NYC Law Department, mirrored locally

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