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GCMS analysis results for sample AE08961, May 7, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08961 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000049584–000049595

Folder label: “GCMS X 4/16/02 A 4/24/02

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NYC 9/11 Public Portal Document

'Data File : C:\MSDCHEM\1\DATA\020424\08961.D Vial: 12 Acq On : 24 Apr 2002 8:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: events.e Quant Time: Apr 26 09:50:52 2002 Quant Results File: SCAN020424.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Wed Apr 24 08:54:34 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1 Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.37 152 9935726 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 38600182 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.46 164 21479260 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 31699748 40.00 ug/1 -0.02 38) Chrysene-dl2 39.93 240 24132823 40.00 ug/1 -0.05 44) Perylene-dl2 43.16 264 15962837 40.00 ug/1 -0.02

System Monitoring Compounds 27) TCMX 27.54 207 1022393 8.46 ug/1 -0.03 Spiked Amount 10.000 Recovery = 84.60% Target Compounds Qvalue 43) Bis(2-ethylhexyl)phthalate 40.53 149 92959 0.21 ug/1 96

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08961.D SCAN020424.M Fri Apr 26 09:52:53 2002 Page 1

NYC-WTC_000049586

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NYC-WTC_000049586Source: NYC Law Department, mirrored locally

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