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GCMS analysis results for sample AE09156, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09156 conducted on May 8, 2002.

NYC-WTC_000046420–000046433

Folder label: “GCMS X 4/17/02 A 4/24 - 4/26/02

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Scanned page image, NYC-WTC_000046422
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\09153.D Vial: 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: events.e Quant Time: Apr 26 14:01:42 2002 Quant Results File: SCAN020424.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Wed Apr 24 08:54:34 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.38 152 9806625 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 37943235 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.46 164 21302406 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 31553743 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 24665862 40.00 ug/1 -0.04 44) Perylene-dl2 43.16 264 16398422 40.00 ug/1 -0.02 System Monitoring Compounds 2 7) TCMX 27.54 207 853564 7.12 ug/1 -0.03 Spiked Amount 10.000 Recovery = 71.20% Target Compounds Qvalue 35) Di-n-butylphthalate 34.81 149 143327 0.15 ug/1 100 43) Bis(2-ethylhexyl)phthalate 40.52 149 226017 0.50 ug/1 95

(#) = qualifier out of range (m) = manual integration (+) = signals summed 09153.D SCAN020424.M Fri May 03 11:00:06 2002 Page 1

NYC-WTC_000046422

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NYC-WTC_000046422Source: NYC Law Department, mirrored locally

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