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GCMS blank analysis results for sample AE06338, May 2 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry blank analysis showing results below method detection limits for organic compounds.

NYC-WTC_000044433–000044446

Folder label: “GCMS X 4/29/02 A 5/1/02

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Scanned page image, NYC-WTC_000044441
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050102\0429LB.D Vial: 10 Acq On 1 May 2002 5:02 pm Operator: Melean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 l-Silacyclo-3-pentene Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.27 ug/L 115277 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Silacyclo-3-pentene 84 C4H8Si 007049-25-4 3 2 lH-Pyrazole, 4,5-dihydro-4,5-dim... 98 C5H10N2 028019-94-5 3 Cyclohexane, methyl- 98 C7H14 000108-87-2 9 4 3-Penten-2-one, 4-methyl-98 C6H10O 000141-7 -7 9 Abundance Scan 330 (5.018 min): 0429LB.D (-318) (-) m/ z 83.10 A 00.00% 55 83

40 98 5000

49 35 4.60 4.80 5.00 5.20 5.40 I I I I I I I I I I I I I I I I ( I 1 I I I TT -mTTTTTTT inip TF m/z 55.10 80.69% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #32988:1-Silacyclo-3-pentene 83

5000 55 4.60 4.80 5.00 5.20 5.40 43 m/z 98.10 53.93% 69 । 50 " " r " 11" ‘ ■ i" " r "11" --- J90.44 TH 77 11'" I" " I' ‘" I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #33297:1H-Pyrazole, 4,5-dihydro-4,5-dimethyl- 83 | I I I I | r i r r I I I I > | I I I | | | |

4.60 4.80 5.00 5.20 5.40 5000 28 42 98 m/z 40.10 48.58% 56

51 , 69 I|।!I!|!>!।|>I ’111. 1111 [ 11111 11 ■ i■ ■ ■■ । " 111"■11■■"11■ 'r"1! m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #116408: Cyclohexane, methyl- 83 4.60 4.80 5.00 5.20 5.40 55 m/ z 84.00 40.61% 5000 41 69 98 "WWMlHWoAps 27

m/z-> -52 + 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 50 , । |i 111 4 3—4++ 77. 4 TTT91 THH+ 11" " i ] i r I > | I I I I | I I I I । I I I | | | r

4.60 4.80 5.00 5.20 5.40

0429LB.D 050102.M Thu May 02 14:53:45 2002 Page 6

NYC-WTC_000044441

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NYC-WTC_000044441Source: NYC Law Department, mirrored locally

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