Calibration data for GCMS analysis of volatile organic compounds recorded on April 22, 2002.
NYC-WTC_000044298–000044303Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\APR1802\7485.D Vial: 18 Acq On : 20 Apr 2002 10:09 am Operator : Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 j MS Integration Params: GOOFY.P Quant Time: Apr 22 12:26 2002 Quant Results File: GCMS84 19 . RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator W/ X Title : 209 625/TCLP calibration table / J ) / N Last Update : Fri Apr 19 14:51:24 2002 v \ / 0 Response via : Initial Calibration DataAcq Meth : GCMS0412
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.21 152 400948 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 1457917 20.00 ug/1 -0.03 17) Acenaphthene-dlO 21.15 164 824878 20.00 ug/1 -0.03 30) Phenanthrene-dlO 25.59 188 1219423 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 795763 20.00 ug/1 -0.04 45) Perylene-dl2 37.87 264 502997 20.00 ug/1 -0.05
System Monitoring Compounds 2 8) TCMX 23.28 209 30787 4.48 ug/L -0.05 Spiked Amount 4.000 Recovery = 112.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 1035 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration 7485.D GCMS0419.M Mon Apr 22 12:27:11 2002 Page 1
NYC-WTC_000044298
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000043498
Calibration table excerpt from GCMS analysis of sample AE07108 showing surrogate recovery data from April 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043514
Calibration table excerpt from GCMS analysis of sample AE07109 showing surrogate recovery data from April 19, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043442
Gas chromatography-mass spectrometry analysis report for sample AE07105 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043427
Gas chromatography-mass spectrometry analysis report for sample AE07068 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043410
Gas chromatography-mass spectrometry analysis report for sample AE07067 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043362
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043378
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011091
Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03075 on March 22, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004706
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010409
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons on February 27, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048523
Instrument scan data for GCMS calibration using deuterated standards on April 4, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022902
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder