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GCMS calibration data for method 508, April 22 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 22, 2002.

NYC-WTC_000044298–000044303

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\APR1802\7485.D Vial: 18 Acq On : 20 Apr 2002 10:09 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 12:26 2002 dQuant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.59 178 155 N.D. 35) Anthracene 0.00 178 0 N.D. 36) Di-n-butylphthalate 27.55 149 4040 N.D. 37) Fluoranthene 29.28 202 292 N.D. 4 0) Pyrene 29.95 202 181 N.D. 41) Butylbenzylphthalate 0.00 149 0 N.D. 42) Benzo(a)anthracene 33.71 228 21649 0.98 ug/1 94 43) Bis(2-ethylhexyl)phthalate 33.86 149 7268 0.36 ug/1 # 97 44) Chrysene 33.71 228 21406 0.97 ug/1 97 46) Di-n-Octylphthalate 35.60 149 5795 N.D. 47) Benzo(b)fluoranthene 36.69 252 8609m 0.45 ug/1 48) Benzo(k)fluoranthene 36.75 252 15489 0.83 ug/1 96 49) Benzo(a)pyrene 37.68 252 2653 N.D. 50) Indeno(1,2,3-cd)pyrene 41.96 276 3749 N.D. 51) Dibenz(a,h)anthracene 42.04 278 2988 N.D. 52) Benzo(g,h,i)perylene 0.00 276 0 N.D. d

(#) = qualifier out of range (m) = manual integration 7485 .D GCMS0419.M Mon Apr 22 12:27:12 2002 Page 2

NYC-WTC_000044299

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NYC-WTC_000044299Source: NYC Law Department, mirrored locally

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