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← Document results/DEP Box 25/GCMS X 4/25/02 A 5/7/02
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GCMS analysis results, sample AE09971, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044071–000044093

Folder label: “GCMS X 4/25/02 A 5/7/02”

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Scanned page image, NYC-WTC_000044085
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial : 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Cyclobutanol, 2-ethyl- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.09 0.30 ug/L 203781 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclobutanol, 2-ethyl- 100 C6H120 035301-43-0 53 2 Hexanal 100 C6H120 000066-25-1 53 3 Hydrazine, butyl-, oxalate (1:1) 178 C6H14N204 006629-62-5 47 4 Hexanal 100 C6H120 000066-25-1 47 Abundance Scan 343 (5,094 min): 9977.D (-338) (-) m/z 44.05 100.00% 44 56 A

5000 129 wAAWMMW Was 72 ‘ I I I ■ I I I I I I I I I I I I I I I I I I I 82 + 35 4.80 5.00 5.20 5.40 ............... I, ,. I । 1 ■ । ■1 I 88 . . . i ' . I t i > . . . I 1 । > > । i-'', । । । , , । । । m/z 56.10 78.78% m/z-> 10___ 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16670: Cyclobutanol, 2-ethyl- 44 57 72 I I 1 [ I I I I 1 *1 _ I _ I I [ I I | I I 5000 29 4.80 5.00 5.20 5.40 m/z 41.0 5 72.12% 82 ,111,1.. 39 1514 -PP m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130

aHWkonn Abundance #110562: Hexanal 44 56

4.80 5.00 5.20 5.40 5000 m/z 57.10 53.00% 27 N 72 82

m/z-> 10 15 20 +130—34140 50.1 50 465 1 ' ' It | । 100 | । > I | I > I ' | r i 60 70 80 90 100 110 120 130 Abundance #1157: Hydrazine, butyl-, oxalate (1:1) । ■ i ■ ■ ■ > i ■ ■ ■ i ■ ■ 1’1*1’ 32 44 4.80 5.00 5.20 5.40 m/z 128.90 38.15% 56 5000 73 88

..................... Ill ' ■ i 1 1 1 ■ i ' 1 1 1 1 1 — ’ I I I < I I I I I I I I I •‘‘‘‘1‘1‘11‘1‘II‘II‘III m/z-> 10 20 30 50 60 70 80 90 100 110 120 130 4.80 5.00 5.20 5.40

9977 .D 050102.M Tue May 07 15:54:23 2002 Page 10

NYC-WTC_000044085

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NYC-WTC_000044085Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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