GCMS analysis results, sample AE09972, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\9972.D Vial : 20 Acq On 7 May 2002 3:11 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetic acid, chloro-, ethyl... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 3.72 0.33 ug/L 265484 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 9 2 Thiophene 84 C4H4S 000110-02-1/5 3 Dicyandiamide 84 C2H4N4 000461-58-5 5 4 Thiophene_____ 84 C4H4S 000110-02-1 5 Abundance Scan 108 (3.714 min): 9972.D (-97) (-) m/z 84.00 100.00% 49 84 43

5000

37 59 ■ ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । 3.40 3.60 3.80 । I ’ । > । । 4.00 mpr .. 11, —.. — 1)1,1/1/11/1/1/1/11/1/1/1/71/1/7/1/1/1/1, m/z 49.10 86.01% m/z-> 10 20 30 40 50) 60 70 80 90 100 110 120 130 M*MMMtat. Abundance 29 #108005: Acetic acid, chloro-, ethyl ester "Www 5000 ■ ■ ■ i ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । । 1 ■ ■ ।

77 3.40 3.60 380 4.00 42 49 __ m/z 43.10 79.97% 14 ........ i............ .| .35 59 65 • I I 88 94 107 122 riII। ii i । i ।r t l"1 1 1 1 1 1,1111 I’I ' 11 I ! ■ ' | ' I'l I | II |'| | U I I | I I , , | ,

m/z->_______ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #116584: Thiophene 84 58 ■ ' ' I 1 ’l ' I 1 ’h I [ I I-I I I I I I I I 45 3.40 3.60 3.80 4.00 5000 m/z 41.05 66.59% 39

26 32 69 -4+ ' pl I I I I I vm I I I I I I I I I I I I ' I I

m/z^10 Abundance 1 ’' i 1 11 11 ■ ■ 20 30 40 50 60 70 80 90 100 110 120 130 wW Yso #116556: Dicyandiamide ■ ■ ■ । ■ ■ ■ ■ । । ■i । > । । । ■ । > । । 43 84 3.40 3.60 3.80 4.00 m/z 86.00 43.70% 5000 68 k/"epyo 56 -1 ' । I । । I । I । r I ' ' ' ‘ I ' 1 1 i ' ' 1 ■ i 1 ‘ 1 1 । 1 ■ ■ ' । 1 r 1 ' । 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 3.40 3.60 3.80 4.00

9972.D 050102.M Tue May 07 15:50:57 2002 Page 6

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