GCMS analysis results for sample AE11930, June 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11930 conducted on June 4, 2002.

NYC-WTC_000013551–000013573

Folder label: “GCMS X 5/22/02 A 5/23/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11930.D Vial: 10 Acq On : 23 May 2002 5:18 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Acetoacetic acid, 1-thio-, . Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.00 0.66 ug/L 388087 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Acetoacetic acid, 1-thio-, S-all... 158 C7H10O2S 015780-65-1 2 2 1-Propene, 1-chloro-, (Z)- 76 C3H5C1 016136-84-8/2 3 3-Hexen-l-ol, acetate, (E)- 142 C8H14O2 003681-82-1 2 4 2-Methyl-pyrrol ine 83 C5H9N 1000143-24-0 2 Abundance Scan 156 (3.996 min): 1193O.D(-155)(-) m/z 43.10 10®.00%

5000 43

82 M 3.60 3.80 4.00 4.20 4.40 0! TUT ■i>■•>।> ■ ■ ■ i ■ ‘ “ i ■ • ■ ■ i ■ • ■ ■ i ■' ■ ■ i ■ ■' ■ i " ■ ■ i ■ ■ •' t m/z 48.10 63.39% niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance 43 #4034: Acetoacetic acid, 1 -thio-, S-allyl ester ./MMMuo. 5000 27 3.60 3.80 4.00 4.20 4.40 69 m/z 41.10 56.75% 59

niz-> 01 --pl 125 158 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ■ i • ■ “ I • ■ ■ ■ i ‘ ■ i ■ i ■ “ ■ i ■1 ■ ■ i ■ “ ' i ■1

Abundance #1588:1-Propene, 1 -chloro-, (Z)- 41 • ! i » > * | i * r i [ . . • ) । ' 3.60 3.80 4.00 4.20 4.40 5000 m/z 44.00 53.09% 76

miz-> 15 01 TIT —ll ■ MI49lp’ ' ■ 61’i ' ■ i 1 I l r i■ ■' ■ i ■ ‘ ■ i ■ ■ ■•i■■■ ■ i “ ■ ■ i ■ ■1' i1■■■i" " i" 10 :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #6004:3-Hexen-1-ol, acetate, (E)- 43 3.60 3.80 4.00 4.20 4.40 67 m/z 81.90 48.51%

U___ 82 5000 27 54

n/z—> O' Immspual lL p1—4 ■ ■11 ■ ■ ■ ‘ i “ " i “ ■ ■ i ■ “ ■ । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 “ ।■ i ■ ■ “ । L 3.60 3.80 4.00 4.20 4.40

11930.D 052202.M Wed May 29 09:50:19 2002 Page 11

NYC-WTC_000013566

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000013566Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE11926, June 2002 · Box DEP Box 15

NYC-WTC_000013476

Laboratory report documenting GCMS analysis of sample AE11926 conducted on June 4, 2002, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.998