GCMS analysis results, sample AE09973, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\9973.D Vial: 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.61 0.30 ug/L 214193 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 38 2 Thiirane, methyl- 74 C3H6S 001072-43-1 9 3 Allyl mercaptan 74 C3H6S 000870-23-5 9 4 Propanoic acid 74 C3H602 000079-09-4 7 Abundance Scan 89 (3.602 min): 9973. D (-85) (-) m/z 74.00 100.00% 7l4

82 5000

35 38 1I 42 47 3.20 A L 1 1 i 1 1 ' ' i 1 1 1 1 i 1 1 1 1 i ' 1 3.40 3.60 3.80 4.00 50 i ‘71’777141171777771 -H 58 11 1 1 ’1 1 ‘ '"’Tm 1 - 351103,1′11* m/ z 82.00 63.05% n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 0 3.20 3.40 3.60 3.80 4.00 88 47 m/z 84.00 49.13%

m/z-> Abundance ■ । ■ ■ ■ ■ i ■ ■ ■ ’ । 15 20 25 ■ t ■ ■ 30 35 40 I I I I I■I

45 50 I I I I I I I [ I ( I I I I I I I I I I >1 I I I I

50 55 #115343: Thiirane, methyl- 60 65 70 75 TIII 80 86 ।1'111'1111 85 90 95 muta,/"p 41 74 ■ ■ i ■ ■ ■ ■ । ' 1 i ■ ■ 1 ■ । ■

3.20 3.40 360 3.80 4.00 5000 m/ z 76.00 37.59% 45

n/z->____ 15 r । ■1 ■111 20 „24273033* +8, 5359 5*64.54711477. 25 30 35 40 45 50 55 60 65 70 75 80 II’’’ 85 rr'111 90 95 Abundance #28161: Allyl mercaptan ■ i 1 ' 1 1 i 1 ' 1 1 i 1 ’ ■ ' i 1 ■ ■ ■ i 1 ■

41 74 3.20 3,40 3.60 3.80 4.00 m/z 47.05 28.46%

5000 45 wupowoos — 3& 1124 1111 11133 1127 1111 11 148 53 56 59 68 71 I I | I I I | I I I I I I I I I | I I rm I I I I I | I i I 1111-111111111/ ' I ' ‘ ' 1 1 ■ । 1 ■'1 ■ r ■_। 1 1 1 1 । "1 1 । 1 r /z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.40 3.60 3.80 4.00

9973.D 050102.M Tue May 07 15:51:53 2002 Page 5

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