GCMS analysis results, sample AE09771, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\9771.D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 2H-Thiopyran, 5,6-dihydro- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T. 4.25 0.26 ug/L 155370 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Thiopyran, 5,6-dihydro- 100 C5H8S 040697-99-2 9 2 Krypton 84 Kr 007439-90-9 5 3 3H-Pyrazol-3-one, 2,4-dihydro-5-... 98 C4H6N20 000108-26-9 3 4 l-Propyn-3-ol 56 C3H40 1000222-14-3 2 Abundance Scan 199 (4.249 min): 9771 D (-196) (-) m/z 98.19 100.00% 35 93 84

5000 49 11 111/1/111"

m/z—> iapuka 43 58 1 I ‘ 1 ‘ 1 ! ' 1 1 ' I ' 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1111111171111/17117 + 88 11’’ ■ * । ■ ■ ■ ■ । 3.80 m/ z 4.00 35.10 4.20 4.40 4.60 97.52% Abundance #43777: 2H-Thiopyran, 5,6-dihydro- 100 NA A

5000 85 54 3.80 4.00 4.20 4.40 4.60 45 67 m/z 84.00 78.05% "**

rnfe-> 30 35 40 —+50 H 45 50 55 59 111111 60 65 70 75 71 "I i I । I । —। n । > p > 11 80 85 90 95 100 105 '11'1'1 i

Abundance #33829: Krypton 84

3.80 4.00 4.20 4.40 4.60 5000 m/z 100.15 56.73%

42 — 80 T-rp-rT-r-p-rr-r-p-rTTp-rT-^^ "It 1111'1' i ■ ■1111' ■ ■ i111' i m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #118423: 3H-Pyrazol-3-one, 2,4-dihydro-5-methyl- 98 3.80 4.00 4.20 4.40 4.60 41 m/ z 84.90 35.61%

5000

56 67 i । । > i I | । । | 1 1 । ' p n ———। n n — TIIT ■ i ■ ■ ■ ■ i ■ - '111 ‘ 11 ■ 11 > I' । • I --- m/z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 3.80 4.00 4.20 4.40 4.60

9771.D 050102.M Tue May 07 15:44:21 2002 Page 10

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