GC/MS reference analysis results, sample AE09681, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAYO6O2\REFA1.D Vial: 17 Acq On 7 May 2002 7:58 am Operator : Sample GC/MS SCAN 4/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 9:17 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 588272 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 2158700 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 1166833 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1671222 40.00 ug/1 -0.01 38) Chrysene-dl2 33.64 240 1045820 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 663221 40.00 ug/1 -0.01

System Monitoring Compounds 2 8) TCMX 23.27 209 42836 7.54 ug/L -0.02 Spiked Amount 10.000 Recovery = 75.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.83 74 139473 8.67 ug/1 97 3) bis(2-Chloroethyl)ether 11.59 93 258940 12.41 ug/1 96 4) 1,3-Dichlorobenzene 12.09 146 225405 12.29 ug/1 98 5) 1,4-Dichlorobenzene 12.24 146 236936 11.83 ug/1 98 6) 1,2-Dichlorobenzene 12.75 146 228784 13.17 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.07 45 535498 12.42 ug/1 98 8) N-Nitroso-di-n-propylamine 13.46 70 195464 12.50 ug/1 99 9) Hexachloroethane 13.60 117 68089 9.05 ug/1 96 11) Nitrobenzene 13.87 77 230916 11.74 ug/1 99 12) Isophorone 14.52 82 565445 14.84 ug/1 97 13) bis(2-Chloroethoxy)methane 15.20 93 315548 13.04 ug/1 100 14) 1,2,4-Trichlorobenzene 15.71 180 187637 12.83 ug/1 99 15) Naphthalene 15.89 128 650664 14.40 ug/1 99 16) Hexachlorobutadiene 16.43 225 71123 10.59 ug/1 99 18) Hexachlorocyclopentadiene 18.63 237 34961 5.91 ug/1 99 19) 2-Chloronaphthalene 19.39 162 405989 15.76 ug/1 98 20) Dimethylphthalate 20.48 163 489334 14.92 ug/1 99 21) 2,6-Dinitrotoluene 20.70 165 90847 12.75 ug/1 96 22) Acenaphthylene 20.66 152 627365 13.53 ug/1 99 23) Acenaphthene 21.23 153 421349 15.49 ug/1 99 24) 2,4-Dinitrotoluene 21.86 165 105491 13.81 ug/1 97 25) Diethylphthalate 22.61 149 476810 16.03 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 215000 15.28 ug/1 99 27) Fluorene 22.75 166 460931 15.90 ug/1 100 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 516039 12.91 ug/L 96 31) N-Nitrosodiphenylamine 23.15 168 139888 12.62 ug/1 98 32) 4-Bromophenyl-phenylether 24.23 248 119074 14.67 ug/1 96 33) Hexachlorobenzene 24.66 284 142978 15.77 ug/1 97 34) Phenanthrene 25.65 178 613616 15.15 ug/1 100

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0501.M Thu May 09 09:18:16 2002 Page 1

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