Analytical report for sample AE09684 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
NYC-WTC_000043768–000043778Folder label: “GCMS X 4/25/02 A 5/7/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\020507\09684.D Vial: 10 Acq On 7 May 2002 9:01 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 .M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Phenethylamine, N-methyl-.b... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
15.46 2.67 ug/1 275033 Naphthalene-d8 16.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenethyl amine, N-methyl-.beta., . . . 399 C18H37NO3Si3 010538-85-9 40 2 Benzoic acid, 2,6-bis[(trimethyl... 370 C16H30O4Si3 003782-85-2 40 3 Trifluoracetyl)-O,O',O''-tris... 495 C20H36F3NO4Si3 054135-51-2 40 4 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 38 Abundance Scan 2107 (15.459 min): 09684.D (-2096) (-) m/z 73.10 100.00% 73
5000 267 355
45 15.20 15.40 15.60 15.80 109133154 193 223 ' ‘ m/z—>______ 50 I ' 1 100 1 1 1 1,1 1 ' 1 1 1 I' 150 200 250 300 350 323 1 1 1 ' i 1 ' ■ ■ i 1 1 1 1 i 1 1 1 1 1 1 400 450 500 m/z 355.10 35.12% Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73
- 5000 355 15.20 15.40 15.60 15.80 m/ z 2 67.00 34.12% 116 147 193 220 267 294 384 — r i ' 1 1 '' i 1 h—pu"ip , । । , । ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ m/z->______ 50 100 150 200 250 300 350 400 450 500 Abundance #27962: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trime... 73 355 .............. ........ ......................
15.20 15.40 15.60 15.80 5000 m/z 356.10 10.73%
147 267 44 95 119 L 179 207 237 i f , 313 ..... ................... 1 ") - m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #27963: N-(Trifluoracetyl)-O,O’,O"-tris(trimethylsilyl)ep... 73 15.20 15.40 15.60 15.80 355 m/z 74.10 9.14% 5000
45 | i, 1 1 i110 140161 184 207 251 281 324 480 TI 1 ' ' 1 'i ■ 1 ' ' i 1 1 1 1 i ■■ i 1 1 1 1 । 1 t 'T ' 1 1 1 1 1 1 1 1 i 1 r ' i 1 ■ ■ ■ i • • ■ ■ । ■ ■n/z-> 50 100 150 200 250 300 350 400 450 500 15.20 15.40 15.60 15.80
09684.D SCAN020507.M Tue May 14 08:40:39 2002 Page 4
NYC-WTC_000043775
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NYC-WTC_000046170
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10131 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046180
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10133 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022516
Reference standard analysis report for nitrosamines and benzene derivatives in sample AE11424 analyzed May 17-21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024935
Chromatogram and integration data from Method 508 GC/MS analysis of sample AE10302 performed on May 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024871
Laboratory report of GCMS analysis for sample AE10246 conducted on May 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024813
Laboratory report of GCMS analysis for sample AE10243 conducted on May 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025613
GCMS analysis report for sample AE11571 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022539
Laboratory report of GCMS analysis for sample AE11426 conducted on May 29, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025592
GCMS analysis report for sample AE11569 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043745
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 25 and May 7, 2002.
Filed in the same folder
NYC-WTC_000043746
Fragmented page containing Method 508 headers and partial text from a DEP laboratory record dated April 2002.
Filed in the same folder
NYC-WTC_000043749
Laboratory report documenting a method blank analysis for GC/MS testing of volatile organic compounds from May 2002.
Filed in the same folder
NYC-WTC_000043756
Calibration data report for sample AE09684 listing response factors and concentrations for target analytes in May 2002.
Filed in the same folder
NYC-WTC_000043760
Reference gas chromatography-mass spectrometry analysis with manual result entry for sample AE09684, detecting multiple organic contaminants.
Filed in the same folder