GC/MS library search results, sample AE08837, April 2002

NYC 9/11 Public Portal Document Llbrary searen compound Keport

Data File : C : \HPCHEM\ 1\DATA\APR2 302\8837.D vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamethyl Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.75 ug/1 138475 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopent as iloxane, decamethyl - 370 C10H3005Si5 000541-02-6 62 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 52 3 N-(Trifluoroacetyl)-N,O,OO''-tetr 553 C22H42F3NO4Si4 000000-00-0 47 4 3,4-Dihydroxymandelic acid, ethyl e 428 C19H3605Si3 000000-00-0 40 Abundance Scan 1064 (14.813 min): 8837.D (-) m/Z 73.00 100.00% 73

355 267 5000

| 1 1 1 I | ! 1l r | 11 I l-“| I J I I | l r

45 14.40 14.60 14.80 15.00 15.20 99 125 154 193 237, [ 323 - I I I' 'l 11 I I I I I I I I i'■ r' v 1 17 i । । । i i m/z 355.05 55.82% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 .................. /..................... 5000 |" i i i i [“i i i D i i । ( j * < F । । । r

14.40 14.60 14.80 15.00 15.20 m/z 267.00 49.94% 207 323, I 1 i ■ 1 ■ i 1 1 1 1 i 1 1 1 1 i 1 1 1 ■ i ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 .................. /.................... ytl I I I [ I I I I I 1fI l 11i I I

14.40 14.60 14.80 15.00 15.20 267 m/ z 356.05 20.48% 5000 179 356

m/z-> I 45

■ 'i 1 50 100 + 147

150 7 —i

200 209 237, '—1—i i i

250 | i r “I

300 | 312 . | I 1 l f pl

350 u I-]

400 I I t I

450 | I I I I

500 or "I "I"' 1 ” |‘ I "I

550 Abundance #60162: N-(Trifluoroacetyl)-N,O,Ol,O"-tetrakis(trimethylsi 73 14.40 14.60 14.80 15.00 15.20 m/z 357.05 13.77% 355 5000

45

m/z-> -L50 1 r-j i 100 i i 147 i । i 150 i 193 i R। 200 i i i k 250 267 r । ( । 300 । । iii pT 350 r ' ' I ' 400 1 ' ' i 1 ' ' ' i ' ■ ' 1 i 1 ' 450 500 538 550 1TT 14.40 14.60 14.80 15.00 15.20 i i । ti i i । i । । i l r

8837.D GCMS0412.M Wed Apr 24 08:36:44 2002 Page 10

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