GC/MS calibration table, sample AE08837, April 2002

Machine-extracted title · confidence 90%

Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.

NYC-WTC_000043699–000043713

Folder label: “GCMS X 4/24/02 A 5/3/02”

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NYC 9/11 Public Portal Document DEaLtii wpOulIU RCPUL L

Data File : C:\HPCHEM\1\DATA\APR2 302\8837.D Vial: 6 Acq On : 23 Apr 2002 7:18 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L Peak Number 9 Propane, 2-methoxy-2-methyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 9.97 0.72 ug/1 103104 1,4-Dichlorobenzene-d4 12.22 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Propane/ 2-methoxy-2-methyl- 88 C5H120 001634-04-4 9 2 5-Hexen-3-ol, 3-methyl- 114 C7H140 001569-44-4 9 3 3,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 9 4 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 8 Abundance Scan 536 (9.966 min): 8837. D (-) m/z 73.00 100.00% 70

5000 43 55 137 ■ • i ■ ■ ■ ■ । । । । ' I ' 9.60 9.80 10.00 10.20 1111 ■111' r „ l, 11 * .... I I 1180 I < I I I 93I J i “J । [ । । । I I | । 15111I I I I I I I I i l I TH 107 r i i | | | । । | | । । । | I I | I m/ z 43.05 36.61% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62967: Propane, 2-methoxy-2-methyl-

5000

41 57 70

A 9.60 9.80 10.00 10.20 34.89% 27 ' ' I 1 15 1 ' I 1 1 ' ' I ' -P— ■ i ■ I ■ • i • ■ ■ • i • TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #3051:5-Hexen-3-ol, 3-methyl- 70 43 4-44m ' i ' 55 9.60 9.80 10.00 10.20 5000 m/ z 57.00 32.57%|

27 81 I I | 66 I i 96 ’ 'I 11 ' i ‘' i' 1II—W1mII"09mmmmPpPPPTD miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5018: 3,4-Dimethyl-5-hexen-3-ol A.................... A / . 3 N 1 i 1 ' ■ ■ i ■ ■ ■ 1 । 1 ' 1 1 i 1 1 1 1 i 1 70 9.60 9.80 10.00 10.20 m/z 136.95 32.36% 43 5000 55

27 ............. .......... ......... 81 99 i । | । r i r [ i i i i । । i ii । i i i r । ill 111111111 ii ( "I‘I‘ । । 111 11 । 11 । 11 11111 ri 11 11 । 111 । 11 11111 —"riv । । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.60 9.80 10.00 10.20

8837.D GCMS0412.M Wed Apr 24 08:36:43 2002 Page 9

NYC-WTC_000043713

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