Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.
NYC-WTC_000043646–000043654Folder label: “GCMS X 4/24/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Qucit LC L — RSDUL L
Data File C:\HPCHEM\1\DATA\MAYO3O2\LB.D Vial: 3 Acq On 3 May 2002 3:58 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 6 9:36 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.20 152 467041 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1704193 40.00 ug/1 -0.03 17) Acenaphthene-dlO 21.14 164 919177 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1259772 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 763711 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 488506 40.00 ug/1 0.00
System Monitoring Compounds 28) TCMX 23.28 209 26253 5.87 ug/L -0.02 Spiked Amount 10.000 Recovery = 58.70%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 193 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 697 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.59 178 338 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0501.M Mon May 06 09:37:15 2002 Page 1
NYC-WTC_000043647
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NYC-WTC_000043164
Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE09450 with semi-volatile organic compounds below detection limits from May 3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043332
Laboratory report documenting GCMS blank analysis for multiple organic compounds on April 24, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044758
Quality control blank analysis for GCMS showing non-detect results for semi-volatile organic compounds with detection limits of 2.0 µg, completed April 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046217
Laboratory data sheet recording GCMS blank analysis parameters for sample AE09579 conducted on May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049302
Laboratory report showing blank analysis results for sample AE08839 with various compounds below detection limits.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039655
Blank check results showing below method detection limits for volatile organic compounds in sample AE06412 on April 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023207
Laboratory report of gas chromatography mass spectrometry blank analysis for volatile organic compounds conducted on May 9, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024187
Laboratory report showing GCMS blank analysis for sample AE10851 on May 20, 2002, listing compounds below method detection limits.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023551
Laboratory report showing GC/MS blank analysis for sample AE09683 with non-detect results for volatile organic compounds.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048881
GCMS blank quality control report for sample AE08684 analyzed on April 22, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048695
Calibration table listing results for various organic compounds including nitrosamines and dichlorobenzenes from April 2002.
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NYC-WTC_000043641
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 24 and May 3, 2002.
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NYC-WTC_000043642
Technical record of GC/MS analytical parameters and sample processing details for the batch dated May 2002.
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NYC-WTC_000043655
Calibration report listing target compounds and their concentrations for the GC/MS analysis performed on May 6, 2002.
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NYC-WTC_000043659
Report detailing the response values for GC/MS reference standards used to verify instrument performance on May 6, 2002.
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NYC-WTC_000043667
Summary of GC/MS analytical results for sample AE08838 processed on May 7, 2002, including surrogate recovery data.
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