Laboratory report for DEP Box 25 showing GCMS blank analysis of sample AE09450 with semi-volatile organic compounds below detection limits from May 3, 2002.
NYC-WTC_000043164–000043173Folder label: “GCMS X 4/19/02 A 5/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY02 02\LB.D Vial: 3 Acq On 2 May 2002 4:42 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 8:13 2002 Quant Results File: GCMS0501.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.19 152 565168 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 2082145 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 1125344 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1557590 40.00 ug/1 -0.01 38) Chrysene-dl2 33.65 240 937606 40.00 ug/1 -0.02 44) Perylene-dl2 37.88 264 596243 40.00 ug/1 0.00
System Monitoring Compounds 2 8) TCMX 23.27 209 38854 7.09 ug/L -0.02 Spiked Amount 10.000 Recovery = 70.90%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.09 146 380 N.D. 5) 1,4-Dichlorobenzene 12.24 146 372 N.D. 6) 1,2-Dichlorobenzene 12.76 146 106 N.D. 7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 13.61 117 303 N.D. 11) Nitrobenzene 13.44 77 757 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 415 N.D. 16) Hexachlorobutadiene 16.43 225 535 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 1318 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 601 N.D.
(#) = qualifier out of range (m) = manual integration LB.D GCMS0501.M Fri May 03 08:13:36 2002 Page 1
NYC-WTC_000043165
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NYC-WTC_000043646
Laboratory report documenting a GC/MS blank run to check for contamination in the analytical system on May 6, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044758
Quality control blank analysis for GCMS showing non-detect results for semi-volatile organic compounds with detection limits of 2.0 µg, completed April 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043036
Ten-page laboratory report showing GCMS blank analysis results for volatile organic compounds with values below detection limits.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043332
Laboratory report documenting GCMS blank analysis for multiple organic compounds on April 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023207
Laboratory report of gas chromatography mass spectrometry blank analysis for volatile organic compounds conducted on May 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048881
GCMS blank quality control report for sample AE08684 analyzed on April 22, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049302
Laboratory report showing blank analysis results for sample AE08839 with various compounds below detection limits.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024187
Laboratory report showing GCMS blank analysis for sample AE10851 on May 20, 2002, listing compounds below method detection limits.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039655
Blank check results showing below method detection limits for volatile organic compounds in sample AE06412 on April 5, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048695
Calibration table listing results for various organic compounds including nitrosamines and dichlorobenzenes from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023551
Laboratory report showing GC/MS blank analysis for sample AE09683 with non-detect results for volatile organic compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000043161
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 19 and May 2, 2002.
Filed in the same folder
NYC-WTC_000043162
Administrative record from DEP Box 25 containing a document identifier with no readable content.
Filed in the same folder
NYC-WTC_000043174
Laboratory report for DEP Box 25 showing GCMS calibration results for sample AE09450 with response factors and MDLs from May 2002.
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NYC-WTC_000043178
Laboratory report for DEP Box 25 showing GCMS reference standard analysis of sample AE09450 with measured concentrations from May 2002.
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NYC-WTC_000043186
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09450 with unknown compounds and surrogate data from May 8, 2002.
Filed in the same folder