GCMS reference standard report, May 6, 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAYO6O2\REF1 .D Vial: 4 Acq On 6 May 2002 12:26 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 8 9:33 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 529010 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1934829 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.13 164 1052358 40.00 ug/1 -0.01 30) Phenanthrene-dlO 25.58 188 1499969 40.00 ug/1 -0.01 38) Chrysene-dl 2 33.64 240 986182 40.00 ug/1 -0.02 44) Perylene-dl2 37.87 264 618561 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.27 209 41886 8.18 ug/L -0.02 Spiked Amount 10.000 Recovery = 81.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.83 74 120352 8.32 ug/1 98 3) bis(2-Chloroethyl)ether 11.59 93 232206 12.38 ug/1 98 4) 1,3-Dichlorobenzene 12.09 146 180482 10.95 ug/1 98 5) 1,4-Dichlorobenzene 12.24 146 190602 10.58 ug/1 99 6) 1,2-Dichlorobenzene 12.75 146 189624 12.14 ug/1 98 7) 2,21 -oxybis(1-Chloropropan 13.07 45 492139 12.69 ug/1 99 8) N-Nitroso-di-n-propylamine 13.46 70 175446 12.48 ug/1 99 9) Hexachloroethane 13.60 117 51305 7.58 ug/1 99 11) Nitrobenzene 13.87 77 212638 12.07 ug/1 100 12) Isophorone 14.52 82 503522 14.74 ug/1 97 13) bis(2-Chloroethoxy)methane 15.21 93 283558 13.08 ug/1 99 14) 1,2,4-Trichlorobenzene 15.71 180 159337 12.16 ug/1 98 15) Naphthalene 15.88 128 584031 14.42 ug/1 99 16) Hexachlorobutadiene 16.43 225 53943 8.96 ug/1 98 18) Hexachlorocyclopentadiene 18.62 237 25909 4.86 ug/1 96 19) 2-Chloronaphthalene 19.38 162 350942 15.10 ug/1 99 20) Dimethylphthalate 20.48 163 434278 14.68 ug/1 100 21) 2,6-Dinitrotoluene 20.69 165 81843 12.73 ug/1 96 22) Acenaphthylene 20.66 152 557843 13.34 ug/1 100 23) Acenaphthene 21.23 153 367492 14.98 ug/1 99 24) 2,4-Dinitrotoluene 21.86 165 94113 13.66 ug/1 99 25) Diethylphthalate 22.61 149 424423 15.82 ug/1 99 26) 4-Chlorophenyl-phenylether 22.77 204 185148 14.59 ug/1 99 27) Fluorene 22.75 166 404261 15.46 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.23 77 447509 12.41 ug/L 97 31) N-Nitrosodiphenylamine 23.16 168 141817 14.26 ug/1 93 32) 4-Bromophenyl-phenylether 24.23 248 103339 14.18 ug/1 97 33) Hexachlorobenzene 24.67 284 126282 15.52 ug/1 100 34) Phenanthrene 25.64 178 544015 14.97 ug/1 99

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0501.M Wed May 08 09:35:05 2002 Page 1

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