GCMS blank analysis results for sample AE09447, May 2002

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GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.

NYC-WTC_000045400–000045410

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAYO8O2\LB.D Vial: 3 Acq On 8 May 2002 11:33 am Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 9 14:29 2002 Quant Results File: GCMS0507.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu May 09 14:27:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0507

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 470036 40.00 ug/1 0.00 10) Naphthalene-d8 15.82 136 1703598 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.13 164 932169 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.57 188 1246625 40.00 ug/1 0.00 38) Chrysene-dl2 33.64 240 618850 40.00 ug/1 0.00 44) Perylene-dl2 37.86 264 356176 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.27 209 29524 6.37 ug/L 0.00 Spiked Amount 10.000 Recovery = 63.70%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis (2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 933 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.66 152 334 N.D. 23) Acenaphthene 21.22 153 322 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 646 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.64 178 494 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0507.M Thu May 09 14:29:48 2002 Page 1

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