GCMS calibration data sheet, April 18, 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\APR18 02\DFTPP2.D Vial: 1 Acq On 19 Apr 2002 12:36 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP2.D

2500000

2000000 4 1500000

1000000

500000

............... 0 । i i I I / [ I I < i | i । i i ) i I I T| i i i f JI................................................... । । । ii । । । । i [ । । । i । i i i ijiii i [ i i n । । i । i 5il r 1 1 i ■ ■ 1 ' 1 1 ' Time-> 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2368 (26.781 min): DFTPP2.D (-) 198

300000 442

200000 69 255 127 51 100000 110 275 224 93 । 167

m/z-> 0 37 1 ■ ।11 40 60 --HH44+4 1*r141 1** pr " . ,11242.1 , j,, 226310323.346 365 383 403 423 —r I > i I । i । r r । 'i । । 'i । i । ii । r । F । । n tn |“i । i" । ■ । “r । i i “u’v 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 2368

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 33.8 122864 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 44.3 161280 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 41.3 150400 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 363904 PASS 199 198 5 9 6.9 25048 PASS 275 198 10 30 23.8 86720 PASS 365 198 1 100 2.4 8736 PASS 441 443 0.01 100 93.5 53632 PASS 442 198 40 110 80.0 291200 PASS 443 442 17 23 19.7 57360 PASS

TTTDD2 n CGMCAAQ M L- 4 1 Q nAA )

NYC-WTC_000043523