Fragmented GCMS document header from April 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\APR23 02\DFTPP.D Vial: 1 Acq On 23 Apr 2002 2:17 pm Operator : Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D 2500000

2000000

1500000

1000000

500000

..... 1.... Orcrunt”u I | i n i | i b > i | i r . i ] i * I > J . .. ... .............. | I I , • | 1 1 • | I ) 11111’1"’’’/’’* TT TT11117‘‘11‘‘‘1‘‘11 TTEETI ‘ ‘‘I’’ 1 I Time~> 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2368 (26.786 min): DFTPP.D (-) 8 300000 C

200000 tn m m ( 0 8

100000 w o m o

to SCM + 3 .8 A10. 0 o 8, a, *. ,0 © CO O <*>C

m/z-> 0 Mu8l++ TTT 4 ' 'I ' ' ++ 8, . J 40 60 80 8-4 HHakri 13_ ‘ 4 "i i । I | । > 1 I | 1 I I T ]' I i 1 । | 1 1 ' 1 | 11 ‘ | 1 1 1 1 11 100 120 140 160 180 200 220 240 260 280 300 320 340 360 . 380 400 420 440 TTT

Spectrum Information: Scan 2368

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 30.4 101808 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 41.5 138944 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 40.3 134656 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 334464 PASS 199 198 5 9 6.4 21360 PASS 275 198 10 30 24.4 / 81456 PASS 365 198 1 100 2.4 8170 PASS 441 443 0.01 100 95.2 53704 PASS 442 198 40 110 89.1 297984 PASS 443 442 17 23 18.9 56424 PASS

DFTPP.D GCMS0412.M Wed Apr 24 11:12:33 2002

NYC-WTC_000046459