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GCMS Method 508 lab analysis data, March-April 2002

Machine-extracted title · confidence 100%

Laboratory analysis worksheet documenting Method 508 GCMS testing parameters including drip rate, volume, and detection counts for sample analysis conducted in March-April 2002.

NYC-WTC_000039640–000039642

Folder label: “GCMS X 3/19/02 A 4/5/02

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Scanned page image, NYC-WTC_000039642
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\APR04 0 5\DFTPP.D Vial: 1 Acq On 5 Apr 2002 9:58 am Operator: Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D

1500000 I 1000000

500000

0- .......... ....... ............................. ‘ I I I I I I I I If I I I 1I I 1 I I I I I ' 1 [.7 I I I { 1111’0 }11E11——1ITI1I11117 TIT । r । . . . . । . . . i | ! I I i~[ i . I I | Time-> 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2372 (26,819 min): DFTPP.D (-) 198 200000 442 150000

69 255 100000 127 51 110 275 50000 224 93 0 37 + 1 up— +144 111' ■ — _ 148 1671811/1241 l — 296 TTprmrrfuTdfunXTErTTTTur 323 346 365 383 403 423 Irr m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 2372

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 32.9 73081 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 44.6 99040 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 41.3 91817 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 222181 PASS 199 198 5 9 6.5 14490 PASS 275 198 10 30 23.7 52685 PASS 365 198 1 100 2.3 5038 PASS 441 443 0.01 100 91.0 30448 PASS 442 198 40 110 76.2 169327 PASS 443 442 17 23 19.8 33456 PASS

DFTPP.D GCMS0408.M Wed Apr 10 11:30:14 2002

NYC-WTC_000039642

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NYC-WTC_000039642Source: NYC Law Department, mirrored locally

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