GCMS calibration data sheet, April 18, 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\APR1802\DFTPP.D Vial: 1 Acq On 18 Apr 2002 11:31 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D

2000000

1500000

1000000

500000

0 ■ 1--- । । i 212 । Pi | I' 1 - r-i"i~i~| i i i i । i i i i । i i i i | । । । । । । । iA । i । । । । । । । । । < । j । । । । । । < । । । । । । ■ । । । ■ । । । > । । । < ■ < । । < । ।

Time-> 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 28.20 28.40 28.60 Abundance Scan 2367 (26.775 min): DFTPP.D 198 250000

200000 442

150000 69 255 127 100000 51 110 275 50000 224 93 423 h J hp TTIr 4---— ++181,1444,24. T11 167 , L 296 310323 346 365 383 403 37 4— rr 0 TUTTnr . 141 ———u——0TutmE-OTTT IIPPur m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Scan 2367

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 35.1 93440 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.7 124192 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 42.9 114088 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 266048 PASS 199 198 5 9 6.6 17464 PASS 275 198 10 30 23.1 61480 PASS 365 198 1 100 2.3 6070 PASS 441 443 0.01 100 93.0 35192 PASS 442 198 40 110 72.9 193984 PASS 443 442 17 23 19.5 37840 PASS

DFTDD n GGMCAA12 M 1- 1 Q nO - A A . 1

NYC-WTC_000043522