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GCMS calibration data for sample AE07108, April 2002

Machine-extracted title · confidence 90%

Calibration table excerpt from GCMS analysis of sample AE07108 showing surrogate recovery data from April 19, 2002.

NYC-WTC_000043498–000043503

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\APR18027108.D Vial: 27 Acq On : 19 Apr 2002 3:38 pm Operator: Sample : GC/MS SCAN 3/26 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.217 775 781 797 rVB 1414939 3598896 68.98% 13.946% 2 15.843 1170 1176 1193 rBV 2210530 4634300 88.83% 17.958% 3 21.149 1748 1754 1767 rBV 2501070 5216993 100.00% 20.216% 4 23.288 1981 1987 1992 rBV 135727 263338 5.05% 1.020% 5 25.592 2231 2238 2250 rBV2 2422021 5074987 97.28% 19.666%

6 33.653 3108 3116 3129 rBV2 1594238 3882093 74.41% 15.043% 7 33.864 3134 3139 3151 rVB 66298 151086 2.90% 0.585% 8 37.876 3568 3576 3588 rBV2 1002967 2984416 57.21% 11.565%

Sum of corrected areas: 25806109

7108.D GCMS0419.M Mon Apr 22 08:34:21 2002

NYC-WTC_000043501

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NYC-WTC_000043501Source: NYC Law Department, mirrored locally

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