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Document / 7 pages

TCLP calibration table review document, April 2002

Machine-extracted title · confidence 100%

Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.

NYC-WTC_000043378–000043384

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1802\7002.D Vial: 20 Acq On : 19 Apr 2002 6:30 am Operator: Sample : GC/MS SCAN 3/26 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.210 338 345 372 rBV 3342070 8554766 100.00% 26.550% 2 12.213 775 781 797 rVB 1426385 3378970 39.50% 10.487% 3 15.848 1171 1177 1193 rBV 2133375 4356304 50.92% 13.520% 4 21.154 1748 1755 1776 rBV 2268379 4912991 57.43% 15.248% 5 23.284 1980 1987 1993 rBV 155797 300159 3.51% 0.932%

6 25.589 2231 2238 2249 rBV2 2194561 4693125 54.86% 14.565% 7 33.649 3108 3116 3134 rBV2 1447039 3448589 40.31% 10.703% 8 37.872 3567 3576 3591 rBV2 855718 2576694 30.12% 7.997%

Sum of corrected areas: 32221598

7002.D GCMS0419.M Mon Apr 22 08:32:51 2002

NYC-WTC_000043381

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NYC-WTC_000043381Source: NYC Law Department, mirrored locally

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