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GCMS analysis report for sample AE07002, April 2002

Machine-extracted title · confidence 100%

GCMS results for sample AE07002 showing surrogate recovery and unknown compounds dated April 29, 2002.

NYC-WTC_000043369–000043377

Folder label: “GCMS X 4/23/02 A 4/24/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\APR2402\7002.D Vial: 7 Acq On : 24 Apr 2002 9:39 pm Operator: Sample : gc/ms scan 4/23 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.182 338 342 369 rBV 846517 1935678 50.74% 9.445% 2 12.212 775 781 796 rBV 1053319 2646618 69.38% 12.914% 3 15.838 1171 1176 1194 rBV 1586390 3371163 88.37% 16.449% 4 21.144 1748 1754 1766 rBV 1916585 3814824 100.00% 18.614% 5 23.283 1979 1987 1992 rBV 184297 350665 9.19% 1.711% 6 25.588 2231 2238 2249 rBV2 1737840 3628211 95.11% 17.703% 7 33.639 3108 3115 3133 rBV2 1179879 2706052 70.94% 13.204% 8 37.871 3567 3576 3603 rBV2 678238 2041171 53.51% 9.960%

Sum of corrected areas: 20494382 7002.D GCMS0412.M Thu Apr 25 11:15:33 2002

NYC-WTC_000043374

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NYC-WTC_000043374Source: NYC Law Department, mirrored locally

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