GCMS sample AE07106 analysis report with surrogate recovery, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR18 02\710 6.D Vial: 25 Acq On : 19 Apr 2002 11:38 am Operator: Sample : GC/MS SCAN 3/26 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L Peak Number 1 3-Penten-2-one, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 7.14 5.16 ug/1 880319 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 (94 2 4-Hydroxy-4-methylpentanone 116 C6H1202 000000-00-0 83 3 Cyclohexane, me t hyl- 98 C7H14 000108-87-2 72 4 3-Hexen-2-one 98 C6H10O 000763-93-9 56 Abundance Scan 228 (7.137 min): 7106.D (-) m/z 82.95 100.00% 55 83

5000 98 43

6.80 7.00 7.20 7.40 i'111 r 1111 Tr++H3E ++47.514 , 62 67 73 77 I i i । I r i । | । I r । । i i i i pi l ri । i-r ! | I ! J ! | | I ! | i I 11" " i'1 m/z 55.00 79.45% mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63217: 3-Penten-2-one, 4-methyl- 55 83

43 98 5000 I * । i i I । । T I 'I I | I I I U I I i i p-

6.80 7.00 7.20 7.40 m/z 98.0.5 45.84% 51 i1'111 - H 67 79 i'1" i " 11111111 I I + I 1111 " i1' I I I I I I I I I I I

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3236:4-Hydroxy-4-methylpentanone 55 83 98 6.80 7.00 7.20 7.40 5000 m/z 42.95 36.78% 43

37 51 i 79 I‘‘‘I t " " 1111' —IIIPTPUTTTT III — I " 111" " i Im..... m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 „ — / _ / Abundance #1326: Cyclohexane, methyl- I I I I I 1 I- 1 1 1 I I I J P—en—- 83 6.80 7.00 7.20 7.40 55 m/z 39.05 26.30%

5000 98 42 27 69 > 1 | ! I । I ! ! ! | I I > I | > । I I I I I I I I I I I I I I i'1,11 111'11 ।1 *111 ' i ■111111 I I I I > I I I I < I I I I I I1"I 1 1 I J" miz- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.80 7.00 7.20 7.40

7106.D GCMS0419.M Mon Apr 22 08:33:57 2002 Page 1

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