Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.
NYC-WTC_000043146–000043160Folder label: “GCMS X 4/18/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File C:\HPCHEM\l\DATA\MAY0102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
25.48 0.54 ug/1 42024 Phenanthrene-diO 25.58
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 38 2 2-Hexenedioic acid,/ bis (trimethylsi 288 C12H2404Si2 055494-10-5 32 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 4-Cyclohexene-l, 2-/dicarboxylic acid 348 C14H25C104Si2 106450-29-7 23 Abundance Scan 2231 (25.482 min): 9398. D (-) m/z 73.10 100.00% 73
5000 147 । 1 । । । । । । । । । T t । । । । । । 1 । । - 221 45 1 1 i ' 1 1 r i ' ■ f ' 1 1 ,11 I 11281 I I I [I I 355 ! LI I 429 I I 25.20 25.40 25.60 25.80 m/z 147.15 22.81% m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 267 TT 1iB, 1 1 i ' 1 5000 25.20 25.40 25.60 25.80 355 429 207 m/Z 221.10 15.31% 45 1 ■ I 1 1 > ' I 1 I 111 J I m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777: 2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- 73 T 25.20 25.40 25.60 25.80 5000 m/z 429.05 8.25% 147 45 — | 112 244 ′ 273 ... .... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 25.20 25.40 25.60 25.80 m/z 74.10 8.06%
5000 147
221 281 327 — | , r 1 I | I I i i । , i I I | I I I I | I r ,i 1 1 ■ i 415 1 1 1 1 i ■ ■ ■ 1 i 519 561 ■ ■' 1 1 i ■ ' 1 1 I ' ' 1 1 I ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 25.20 25.40 25.60 25.80
9398.D GCMS0501.M Thu May 02 12:04:41 2002 Page 9
NYC-WTC_000043159
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NYC-WTC_000043079
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045223
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10432 conducted on May 20, 2002.
Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043058
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09391 with unknown compounds and surrogate data from May 8, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043112
Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09395 with unknown compounds and surrogate data from May 9, 2002.
1 shared non-person entities · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044723
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023363
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023148
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
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NYC-WTC_000043032
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 18 and May 1, 2002.
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NYC-WTC_000043033
Three-page laboratory record detailing GCMS method parameters including drip rates and volumes for samples analyzed in May 2002.
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Four-page document containing GCMS calibration data and response factors for various chemical compounds analyzed on May 1, 2002.
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Eight-page laboratory report showing GCMS reference analysis results for volatile organic compounds analyzed on May 1, 2002.
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