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ICPMS daily performance check report, April 23, 2002

Machine-extracted title · confidence 95%

Daily instrument performance verification log for ICPMS analysis including intensity and standard deviation data for multiple elements.

NYC-WTC_000040976–000041063

Folder label: “ICPMS 4/23/02

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NYC 9/11 Public Portal Document

WESTCHESTER COUNTY DEPT OF LABS AND RESEARCH Method 200.8 - Summary Report Sample ID: AE08839 Sample Date/Time: Tuesday, April 23, 2002 10:26:25 Sample Type: Spike -1 Sample Description: MSD Number of Replicates: 3 Method File: d:\elandata\Method\NYC.mth Dataset File: d:\elandata\Dataset\new york city\AE08839.667 Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit Be 9 19291.312 2.048 0.042 55.95789 0.65 ug/L Se-1 45 464602.889 1.397 464602.889 ug/L Cr 52 424708.396 2.306 0.898 49.25539 2.13 ug/L Cr 53 51047.769 0.720 0.108 49.97902 1.18 ug/L Mn 55 906011.481 1.238 1.948 68.82078 1.13 ug/L Ni 60 105142.854 2.643 0.226 50.16128 1.27 ug/L Cu 63 264420.023 1.255 0.568 55.48031 0.30 ug/L Cu 65 131160.461 1.271 0.282 55.11334 0.23 ug/L Zn 66 83803.690 1.018 0.912 54.80500 0.41 ug/L Zn 67 15085.658 1.107 0.164 53.86114 0.56 ug/L Zn 68 62944.871 2.401 0.685 55.02245 1.70 ug/L > Ge 72 91060.411 1.303 91060.411 ug/L As 75 95416.730 0.277 1.047 53.38877 1.25 ug/L Se 77 9457.130 1.221 0.103 57.67144 1.61 ug/L Se 82 11230.044 0.695 0.122 56.54860 1.99 ug/L Ag 107 463648.645 2.466 0.374 49.27239 2.07 ug/L Cd 111 126788.074 1.824 0.102 51.24537 1.37 ug/L Cd 114 296575.211 2.632 0.239 50.96494 2.36 ug/L in 115 1238864.833 0.507 1238864.833 ug/L Sb 121 434057.627 0.070 0.350 51.52532 0.46 ug/L Sb 123 335447.848 1.141 0.271 51.38622 0.73 ug/L Ba 135 165512.479 0.866 0.095 65.11577 1.58 ug/L Ba 137 288306.093 1.506 0.166 64.76341 0.92 ug/L > Tb 159 1734995.287 1.018 1734995.287 ug/L Ho 165 1715845.225 1.987 -0.003 ug/L Hg 201 4530.841 0.720 0.003 4.09229 0.32 ug/L Hg 202 10073.681 2.551 0.006 3.89754 2.63 ug/L TI 205 1094694.180 0.889 0.631 47.01399 0.89 ug/L Pb 208 1480570.920 1.225 0.852 47.38375 0.27 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff ' Be 9 111.925 > Sc-1 45 100.053 Cr 52 97.970

Sample ID: AE08839 Report Date/Time: Tuesday, April 23, 2002 10:29:03 Page 1

NYC-WTC_000041019

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NYC-WTC_000041019Source: NYC Law Department, mirrored locally

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